Physics Lab Equipment

LEAI-15 Microwave Electron Spin Resonance Apparatus

LEAI-15 Microwave Electron Spin Resonance Apparatus

Note: oscilloscope not included

Features

  • Simple structure

  • Ample experimental examples

  • Stable performance






Introduction

Electron spin resonance, also known as electron paramagnetic resonance (EPR), refers to the phenomenon that a resonance transition between magnetic energy levels occurs when the electron spin magnetic moment is impacted by an electromagnetic wave of specified frequency in a magnetic field. This phenomenon can be observed in paramagnetic substances with unpaired spin magnetic moment (i.e. compounds containing unpaired electrons). Thus, electron spin resonance is an important method to reveal the microstructure of a substance by probing the unpaired electrons in the material and analyzing how they interact with surrounding atoms. This method has high sensitivity and resolution, and it is a nondestructive detection technique for analyzing the internal structure of materials. This technique has been widely used in physics, chemistry, biology and medicine, and other fields of study.

 

This apparatus of electron spin resonance in microwave band is specially designed for teaching advanced physics at universities and colleges. Using this apparatus, the following experiments can be conducted:

 

1. Study and acknowledge electron spin resonance phenomenon.

2. Measure Lande's g-factor of DPPH sample.

3. Learn how to use microwave devices in EPR system.

4. Understand standing wave by changing resonant cavity length and determine waveguide wavelength.

5. Measure standing wave field distribution in resonant cavity and determine waveguide wavelength.


Specifications

Microwave System
Short-circuit pistonadjustment range: 30 mm
SampleDPPH powder in tube (dimensions: Φ2×6 mm)
Microwave frequency metermeasurement range: 8.6 GHz ~ 9.6 GHz
Waveguide dimensionsinner: 22.86 mm × 10.16 mm
Magnetic Field
Output voltage and accuracyMax: ≥ 20 V, 1% ± 1 digit
Output current range and accuracy0~2.5 A, 1% ± 1 digit
Stability≤ 1x10-3+5 mA
Sweep Field
Output voltage ≥ 6 V
Output current range0.2 ~ 0.7 A
Phase adjustment range≥ 180°
Scan output
BNC connector, saw-tooth wave output 1~10 V
Solid State Microwave Signal Source
Frequency
8.6 ~ 9.6 GHz
Frequency drift
≤ ± 5×10-4/15 min
Working voltage
~ 12 VDC
Output power
> 20 mW under equal amplitude mode



Operation mode & parameters

Equal amplitude

Internal square-wave modulation

Repetition frequency: 1000 Hz

Accuracy:   ± 15%

Skewness: < ± 20%

Voltage standing wave ratio
< 1.2
Waveguide dimensions
inner: 22.86 mm × 10.16 mm


Parts List

DescriptionQty
Main Controller1
Electromagnet1
Support Base3
Microwave System1 set (including various microwave components, source, meters, etc)
DPPH Sample1
Cable7
Instructional Manual1


      Apparatus of Microwave Electron Spin Resonance.png

Diagram of apparatus


         LEAI-15 Microwave Electron Spin Resonance Apparatus.png

  LEAI-15 Microwave Electron Spin Resonance.jpg

(c)

Waveform of EPR signal


     LEAI-15 Microwave Electron Spin Resonance Apparatus.png

Standing wave distribution in cavity


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